聚甲醛纤维的一步法制备及其性能研究Preparation and Properties of Polyoxymethylene Fiber by One Step Method
李建华,杨胜林,汪晓东
LI Jian-hua,YANG Sheng-lin,WANG Xiao-dong
摘要(Abstract):
采用自制的熔融纺丝一体化设备,使用不同熔融指数的聚甲醛的共混料为原料,通过DSC、TGA等测试以及纺丝工艺过程的分析,得出了最佳的原料配比和熔融纺丝工艺。研究了牵伸倍数对聚甲醛纤维拉伸强度的影响,结果表明:在10倍牵伸下,可以制备出拉伸强度为6.2 cN/dtex的聚甲醛纤维。
Using the mixed materials of polyoxymethylene with different melting indices as raw materials,polyoxymethylene fibers were prepared through the integrated equipment of self-made melt spinning. The best material ratio and spinning process were obtained by DSC and TGA tests and the spinning process analysis. The effects of draw ratio on the tensile strength of polyoxymethylene fibers were studied, and polyoxymethylene fiber with a tensile strength of 6.2 cN/dtex could be prepared by stretching 10 times.
关键词(KeyWords):
聚甲醛共混料;聚甲醛纤维;熔融纺丝;性能
polyoxymethylene mixed material;polyoxymethylene fiber;melt spinning;property
基金项目(Foundation):
作者(Author):
李建华,杨胜林,汪晓东
LI Jian-hua,YANG Sheng-lin,WANG Xiao-dong
DOI: 10.16090/j.cnki.hcxw.2019.09.004
参考文献(References):
- [1]李相明,覃俊,何勇,等.高性能聚甲醛纤维的研究进展与应用[J].合成纤维,2008,37(12):5-9.
- [2]马承银.聚甲醛单丝[J].合成纤维,1993,22(1):38-40.
- [3]刘露,侯帅,吴静,等.聚甲醛纤维增强混凝土抗折性能研究[J].武汉纺织大学学报,2013,26(3):35-38.
- [4]田国峰,李建华,战佳宇,等.聚甲醛纤维对砂浆性能的影响研究[J].混凝土与水泥制品,2017(7):51-54.
- [5]张丽辉,刘建忠,周华新,等.聚甲醛纤维对混凝土性能的影响[J].混凝土与水泥制品,2018(1):58-62.
- [6]贺溥.聚甲醛-新合成纤维的原料[J].高分子通讯,1958(2):136-138.
- [7]CLARK E S,SCOTT L S.Superdrawn crystalline polymers:A new class of high-strength fiber[J].Polymer Engineering and Science,1974,14(10):682-686.
- [8]FANG X D,WYATT T,SHI J,et al.Fabrication of high-strength polyoxymethylene fibers by gel spinning[J].Journal of Materials Science,2018,53:11901-11916.
- [9]金旺.熔融静电纺制备聚甲醛纤维的工艺及其性能研究[D].北京:北京化工大学,2018.
- [10]WILLIAMS A G.Process for preparing high tenacity Polyoxymethylene fibers:United States,3536219[P].1970 10-27.
- [11]王焕莲,兰建武,刘波,等.聚甲醛的熔融纺丝温度[J].合成纤维,2009,38(4):34-37.
- [12]文珍稀,叶敏,彭刚,等.聚甲醛纤维的制备及其力学性能研究[J].合成纤维,2011,40(1):24-27.
- [13]大川秀俊.聚甲醛树脂纤维的制造方法:101096784B[P].2011-11-23.
- [14]WANG Y T,ZHAO W W,WANG X D,et al.Preparation,mechanical properties and microstructure of polyoxymethylene fiber through melt spinning and hot drawing by using injection-molding grade resins[J].Fibers and Polymers,2016,17(9):1464-1474.
- [15]王亚涛.聚甲醛的改性、加工及应用研究[D].北京:北京化工大学,2017.