低温氨气等离子体对芳纶表面的改性The Study of Low Temperature Ammonia-Plasma Treatment on Surface Modification of Aramid Fiber
李铉喆,李爽,荣怀苹,韩克清,余木火
LI Xuan-zhe,LI Shuang,RONG Huai-ping,HAN Ke-qing,YU Mu-huo(State Key Laboratory for Modification of Chemical Fibers and Polymer Materials
摘要(Abstract):
采用氨气等离子体对芳纶表面进行改性,用X-射线光电子能谱、场发射扫描电子显微镜、力学性能测试等手段对改性前后纤维表面的元素组成、形貌及其拉伸强度进行表征,并进一步通过微脱黏方法分析了等离子体处理条件对芳纶/环氧树脂复合材料界面黏结强度的影响。结果表明:芳纶经表面改性后,其表面极性官能团、表面粗糙度均有所增加,同时与环氧树脂基体的界面黏结强度明显增加。
Aramid fiber surface was modified by ammonia-plasma treatment.The fiber surface chemical composition and surface morphology before and after plasma treatment were characterized by X-ray photoelectron spectroscopy and field emission scanning electron microscope,respectively.The effects of plasma treatment time on the interfacial adhesion of aramid fibers/epoxy resin composites were investigated by the microbond test.The results showed that the content of nitrogen increased obviously,and surface roughness of fiber also increased owing to the ammonia-plasma treatment.The interfacial adhesion of aramid fiber/resin was enhanced.
关键词(KeyWords):
芳纶;氨气等离子体处理;改性
aramid fiber,ammonia-plasma treatment,modification
基金项目(Foundation): 国家重点基础研究发展计划(2011CB606101)
作者(Author):
李铉喆,李爽,荣怀苹,韩克清,余木火
LI Xuan-zhe,LI Shuang,RONG Huai-ping,HAN Ke-qing,YU Mu-huo(State Key Laboratory for Modification of Chemical Fibers and Polymer Materials
DOI: 10.16090/j.cnki.hcxw.2013.03.010
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- 李铉喆
- 李爽
- 荣怀苹
- 韩克清
- 余木火
LI Xuan-zhe - LI Shuang
- RONG Huai-ping
- HAN Ke-qing
- YU Mu-huo(State Key Laboratory for Modification of Chemical Fibers and Polymer Materials
- 李铉喆
- 李爽
- 荣怀苹
- 韩克清
- 余木火
LI Xuan-zhe - LI Shuang
- RONG Huai-ping
- HAN Ke-qing
- YU Mu-huo(State Key Laboratory for Modification of Chemical Fibers and Polymer Materials