聚对苯二甲酸丁二酯牙刷丝表观改善处理工艺研究The Research on Improving the Surface of PBT Toothbrush Filament
田明华,夏发明,王安怡,王晓广
TIAN Ming-hua,XIA Fa-ming,WANG An-yi,WANG Xiao-guang
摘要(Abstract):
对聚对苯二甲酸丁二酯(PBT)牙刷丝进行碱处理来改善丝体表面形貌,得到磨尖丝。用显微镜观察反应前后丝端形貌的变化,分析了磨尖丝的形成原因。用PBT碱水解的理论分析计算并结合丝体减量率的变化,探讨了影响磨尖丝尖峰质量的因素,得出当反应温度为120℃、碱处理液质量分数为40%、反应时间为60~90 min时可以获得较为理想的磨尖效果。
PBT toothbrush filament is treated with alkaline to improve the surface form of the filament to ob-tain tapered filament.The difference of the surface form has been observed before and after the reaction.The tapered filament formation mechanism is analyzed.The major factors which affect the cutting-edge ofthe tapered filament are also discussed.Through the theoretical analysis and calculation of PBT alkaline hy-drolysis reaction and combined with the change of weight loss of filament,the ideal form of cutting-edge ofthe tapered filament is found when the reaction temperature is 120 ℃,the concentration of alkali treatmentfluid is 40%,the reaction time is 60~90 minutes.
关键词(KeyWords):
PBT;碱处理;磨尖丝
polybutylece terephthalate;alkaline treatment;tapered filament
基金项目(Foundation): 武汉纺织大学研究生创新团队项目(201607057)
作者(Author):
田明华,夏发明,王安怡,王晓广
TIAN Ming-hua,XIA Fa-ming,WANG An-yi,WANG Xiao-guang
DOI: 10.16090/j.cnki.hcxw.2016.09.005
参考文献(References):
- [1]韩亚东.合成纤维的后起之秀——PBT纤维[J].合成纤维,1987,16(4):39-41.
- [2]黄新宇.牙刷溯源[J].文献,1999(4):257-259.
- [3]VERSTEEG PA,PISCAER M,ROSEMA NA,et al.Tapered toothbrush filaments in relation to gingival abrasion,removal of plaque and treatment of gingivitis.[J].International Journal of Dental Hygiene,2008,6(3):174-182.
- [4]KWEON Young Jun.Tapered toothbrush bristle and toothbrush with said bristles,and methods for producing the same:US,6090488[P].1998-8-21.